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Beilstein J. Org. Chem. 2022, 18, 1454–1456, doi:10.3762/bjoc.18.150
Graphical Abstract
Scheme 1: a) Mechanochemical PEG-400-assisted halogenation of phenols and anilines using NXS. b) Halogenation...
Scheme 2: Mechanochemical palladium-catalyzed borylation protocol of aryl halides.
Scheme 3: 1,2-Debromination of polycyclic imides, followed by in situ trapping of the dienophile by several d...
Scheme 4: Synthesis of g-h-PCN from sodium phosphide and trichloroheptazine mediated by mechanochemistry.
Scheme 5: Mechanochemical intra- and intermolecular C–N coupling reactions using DDQ as an oxidant.
Beilstein J. Org. Chem. 2019, 15, 1154–1161, doi:10.3762/bjoc.15.112
Figure 1: A: Mechanochemical polymerization of BCMBP (4,4’-bis(chloromethyl)-1,1’-biphenyl) towards the porou...
Figure 2: A: IR spectra of the monomer BCMBP and NG-HCP showing a decrease of the C–Cl vibration after the re...
Figure 3: A: Evolution of pressure in the course of the reaction measured by the GTM system. The addition of ...
Figure 4: The correlation between the liquids’ boiling point and the SSA of the polymer. In general, a lower ...
Figure 5: Physisorption isotherms of benzene vapour at different temperatures on HCP synthesised classically ...
Figure 6: Physisorption isotherms of cyclohexane on mechanochemically synthesised HCP at temperatures 288, 29...
Beilstein J. Org. Chem. 2017, 13, 1332–1341, doi:10.3762/bjoc.13.130
Figure 1: Synthesis of hierarchical porous carbons by mechanochemical polymerization of ethylene glycol (EG) ...
Figure 2: Infrared spectra of the monomers ethylene glycol (EG, blue) and citric acid (CA, green blue), the m...
Figure 3: SEM (A) and TEM (B) images of the Carb-SF-3 sample.
Figure 4: XRD-pattern of the polymeric precursor (Polymer-SF-3, orange), the carbonized composite (Comp-SF-3,...
Figure 5: Nitrogen physisorption isotherms for carbon samples achieved from (A) different amounts of ethylene...
Figure 6: Volume histogram of the different samples calculated using a QSDFT-kernel for slit, cylindrical and...
Figure 7: Cyclic voltammograms performed with different scan rates in (A) 1 M TEA-BF4 (ACN) and (B) EMIM-BF4;...